Malvern Panalytical - Empyrean

X-ray Diffractometer

New multi-functional hard radiation XRD system allowing the study of advanced materials under in-service and extreme conditions.

  • Partner:The University of Sheffield
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Detailed Description

A unique aspect of this equipment is the provision of access to high energy X-rays (Ag – 22keV) which will prove transformative in bringing synchrotron X-ray scattering techniques within reach of the laboratory.

With its pre-aligned Fast Interchangeable X-ray modules for optics and stages, the diffractometer can be reconfigured simply and rapidly, allowing users to switch between different applications in a matter of minutes.

Uses/Applications

The use of hard radiations enables:

  1. Total scattering studies of local atomic environments in both amorphous or crystalline materials
  2. High pressure studies using a diamond anvil cell
  3. Operando diffraction studies of coin or pouch cell type battery devices, so that electrochemical processes and changes in the crystal structure of an electrode material can be followed while e.g. a battery is being (dis)charged.

With its sample stage for big, bulky samples, the Empyrean is also the go-to machine for samples that are heavy (up to 5 kg) or irregularly shaped.

The Empyrean has a host of other applications under development also, so watch this space for more information.

Features

The emphasis for the Empyrean is on advanced characterisation techniques that have historically only been available at central facilities, such as synchrotrons, with long wait times and tricky application procedures to navigate.

For example, the Empyrean brings total scattering and operando diffraction experiments on real devices within easy reach.